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The available fractions of Cu, Zn, Pb, and Cd were extracted with a DTPA 0.005 M, CaCl2 0.01 M, and triethanolamine 0.1 M solution and measured with an ICPOES spectrometer (Optima 8300, Perkin Elmer, Waltham, USA) equipped with a cyclonic nebulizer, using the following wavelengths: Cu = 324.752 nm, Zn = 213.857 nm, Pb = 220.353 nm, Cd = 226.502 nm.
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For this section of the laboratory experiment, a metal (Cu, 99.3%) and three metal alloys (α-brass [64.5% Cu, 35% Zn, 1% Pb], aluminum 6061, and steel 1045) were subjected to uniaxial tension using the Instron Model 4505. The samples were dog-bone structures to localize the point of failure to the center of the samples during testing (Fig. 2.1).
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